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PHOTOCHEMICAL PREPARATION OF A BICYCLIC LACTONE
   
Document Number
US Patent 3627660
Issued Date
December 14, 1971
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Abstract
Synthesis of cis 2-(1'-methyl-2'-isopropenylcyclobutyl)ethanol, a component of the boll weevil sex attractant, and intermediates therefor, in which 5-hydroxy-pent-2-ynoic acid ester or ethers thereof is methylated followed by cyclization to yield 3-methylpent-2-eno-5-lactone which is irradiated in presence of ethylene to yield 2,3-cycloethylene-3-methylpentano-5-lactone which is cleaved and converted into 2-(1'-methyl-2'-isopropenylcyclobutyl)ethanol.
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Number of Claims:
6
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Owner
Zoecon Corporation (Palo Alto, CA)
Published
December 14, 1971
Application Number
04/883,301
Filed
December 8, 1969
US Classification
426/125   426/310 426/573 426/616
Int'l Classification
A23B   7/16   (20060101)   A23B   7/00   (20060101)   A23L   1/00   (20060101)   A23L   1/212   (20060101)  
USPTO Field of Search
260/343   204/158   204/162  
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Description
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