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Process for producing an expandable silicone resin
   
Document Number
US Patent 4467053
Issued Date
August 21, 1984
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Abstract
A process for the production of an expandable silicone resin includes reacting a substantial amount of the silanol (SiOH) groups present in the resin to form siloxane bonds and water, and heating the resin to a temperature above the resin's melting point, at which chemical reaction (condensation) of the silanol groups occur. The reaction increases the molecular weight of the resin and decreases the amount of water that must be removed during a subsequent foaming step, thereby controlling the rate and extent of foaming which can occur. The resin is solidified, pulverized and size-reduced to a powder form. The resin powder is blended with a minor amount of a particulate inert filler which is coated with a silicone resin curing catalyst and also with a minor amount of blowing agent (powder). The dry powder blend is then thermally fused for a closely-controlled, short duration, time at a temperature near the lower end of the blowing agent's gas-generating temperature range. The fused mass is ground to a powdered form to produce an expandable resin.
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Number of Claims:
12
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Owner
Rosemount Inc. (Eden Prairie, MN)
Published
August 21, 1984
Application Number
06/566,276
Filed
December 28, 1983
US Classification
521/128   521/129 521/154 521/77
Int'l Classification
C08J   9/10   (20060101)   C08J   9/02   (20060101)   C08J   9/00   (20060101)  
Examiner
Attorney/Law Firm
USPTO Field of Search
521/129   521/154   521/128  
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