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Process for producing dianthraquinone-N,N'-dihydrazine and its chlorination product
   
Document Number
US Patent 4628091
Issued Date
December 9, 1986
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Abstract
A process for producing dianthraquinone-N,N'-dihydrazine or its chlorination product, which comprises condensing 1-aminoanthraquinone at an elevated temperature in the presence of 1,3-dimethyl-2-imidazolidinone using an oxidizing agent and an alkaline condensing agent, and subjecting the resulting condensation product to a treatment known per se.
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Number of Claims:
4
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Published
December 9, 1986
Application Number
06/620,398
Filed
June 13, 1984
US Classification
544/339   544/341
Int'l Classification
C09B   5/48   (20060101)   C09B   5/00   (20060101)  
Examiner
Attorney/Law Firm
Priority Data
Jun 16, 1983 [JP] 58-106789 Feb 27, 1984 [JP] 59-34405
USPTO Field of Search
544/339   544/341  
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7,16-Dichlorodianthraquinone-N,N'-dihydroazine (I) ##STR1## is prepared by condensing 1-amino-3-chloroanthraquinone (II) in the presence of an alkaline condensing aid, of an oxidizing agent and of a urea derivative (III) ##STR2## (R: identical or different alkyl groups having 1 to 4 carbon atoms, which may be joined together to form a 5- or 6-membered ring that contains the urea group).

5350853 - Preparation of dianthraquinone-N,N'-dihydroazine and its chlorination products - Owned by BASF Aktiengesellschaft (Ludwigshafen,DE)

A process for preparing dianthraquinone-N,N'-dihydroazine (I) ##STR1## and its chlorination products (Ia) ##STR2## where n is 1 or 2, by condensation of 1-aminoanthraquinone (II) in the presence of an alkaline condensing aid, an oxidizing agent and a cyclic urea derivative at from 80.degree. to 150.degree. C. and subsequent purification and/or chlorination comprises using N,N'-dimethylpropyleneurea as the urea derivative.

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