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Latent-image control of lithography tools    

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United States Patent5124927   
Link to this pagehttp://www.wikipatents.com/5124927.html
Inventor(s)Hopewell; William D. (Ridgefield, CT); Jackson; Robert R. (Millbrook, NY); Shaw; Jerry C. (Ridgefield, CT); Van Kessel; Theodore G. (Millbrook, NY)
AbstractMeasurement apparatus and procedure for use with lithographic equipment is provided for the construction of electronic and other devices wherein a photoresist is deposited as a layer upon a substrate. A Nomarski differential interference contrast microscope in conjunction with a scanned image detector is employed to examine verification marks produced by projection of an overlay, such as the mask or reticle, upon the photoresist layer. The projection results in a production of verification marks in the form of a latent image which, while invisible with conventional viewing means, can be viewed by phase-contrast imaging employing differential phase shift. Various characteristics of the resultant image are employed to align secondary verification marks with primary verification marks previously provided on the substrate, and to allow for a checking of line width, dosage, focusing, temperature control, and global alignment. Observation of the photoresist is accomplished with radiation at lower frequency than the exposure radiation, the latter being significantly absorbed, by the photoresist, the photoresist being transparent to the observation radiation to permit reflection from top and bottom surfaces of the photoresist.
   














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Inventor     Hopewell; William D. (Ridgefield, CT); Jackson; Robert R. (Millbrook, NY); Shaw; Jerry C. (Ridgefield, CT); Van Kessel; Theodore G. (Millbrook, NY)
Owner/Assignee     International Business Machines Corp. (Armonk, NY)
Patent assignment
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Publication Date     June 23, 1992
Application Number     07/488,342
PAIR File History     Application Data   Transaction History
Image File Wrapper   Patent Term   Fees
Litigation
Filing Date     March 2, 1990
US Classification     700/121 250/491.1 356/394 356/401 702/94 716/21
Int'l Classification     G06F 015/46
Examiner     Ruggiero; Joseph
Assistant Examiner    
Attorney/Law Firm     Perman & Green
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Parent Case    
Priority Data    
USPTO Field of Search     364/468 364/474.02 364/488 364/489 364/490 364/491 364/559 250/491.1 250/397 250/398 356/372 356/394 356/389 356/397 356/400 356/401 356/349 356/359 430/394 430/326 430/311 430/30 430/935 378/34 378/35 355/43 355/53
Patent Tags     latent-image control lithography tools
   
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5048967
Suzuki
356/401
Sep,1991

[0 after 0 votes]
4984890
Tojo
356/509
Jan,1991

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4834540
Totsuka
356/401
May,1989

[0 after 0 votes]
4814829
Kosugi
355/43
Mar,1989

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4794426
Nishi
355/43
Dec,1988

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4788117
Cuthbert
430/30
Nov,1988

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4766311
Seiler
250/252.1
Aug,1988

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4758094
Wihl
356/394
Jul,1988

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4748335
Lindow
250/559.22
May,1988

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Suwa
356/401
May,1988

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4727381
Bille
347/234
Feb,1988

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4707610
Lindow
250/559.22
Nov,1987

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4701859
Matsuyama
382/144
Oct,1987

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4640619
Edmark, III
356/625
Feb,1987

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4559603
Yoshikawa
716/5
Dec,1985

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What is claimed is:

1. A method of controlling a lithographic tool operating on a surface of a workpiece, the method comprising steps of:

observing the surface of said workpiece; and

wherein said observing comprises:

viewing adjacent sites at a first location on said surface with separate beams of radiation to obtain data of said surface by differential phase shift induced on said beams by reflection from said surface; and

converting said differential phase shift to amplitude data to produce an image point of said first location;

said method further comprising steps of

repeating said observing step at additional locations spaced from said first location to obtain further image points, all of said image points constituting detected image of points on said surface;

providing a reference image pattern; and

correlating detected image with said reference image by use of an edge correlation sum.

2. A method of controlling a lithographic tool having an exposure head and a microscope for processing a wafer having a plurality of fields containing product areas, said wafer being covered with a layer of photoresist, the method providing for a correction of exposure dosage of the photoresist, the method comprising steps of:

exposing a number of said fields, said exposing producing a latent image in said photoresist for each of said number of fields;

moving said wafer to a microscope operative to obtain image data of said photoresist by differential phase shift;

measuring amplitude obtained from the differential phase shift across latent images for each of said number of fields, said step of exposing producing a change of thickness in said photoresist;

obtaining previously measured photoresist thickness data for all of said fields;

calculating exposure correction;

moving the wafer back to the exposure head; and

exposing said photoresist with a further dosage of radiation to adjust the thickness of the photoresist.

3. a method of controlling a lithographic tool having a microscope and an exposure head for processing a wafer, the wafer having a coating of photoresist and comprising a plurality of fields each of which includes a product area, the method providing for a correction of focus of the exposure head, the method comprising steps of:

exposing a number of the fields with stepped focus;

moving said wafer to said microscope, said microscope being operative to produce a detected image of a latent image by differential phase shift;

measuring points of the detected image across the latent image for each cf said number of fields;

calculating a best focus position;

returning the wafer to said exposure head;

adjusting said focus; and

exposing the photoresist by said exposure head with a new value of focus.

4. A method of controlling a lithographic tool having a microscope and an exposure head for processing a wafer, the wafer having a coating of photoresist and comprising a plurality of fields each of which includes a product area, the method providing for a measuring of line width in a latent image in said photoresist, the latent image in the photoresist being produced by exposure of the photoresist, the method comprising the steps of:

exposing a number of said fields with step exposure and focus, the exposure producing a latent image in the photoresist;

moving the wafer to said microscope;

measuring a distance between each position of image points lying on each side of a line in said latent image to obtain a measure of the line width;

calculating a best focus and an exposure combination by comparison of the line width with a line-width set point;

returning the wafer to said exposure head;

setting a new focus and amounts of exposure at said exposure head; and

exposing the photoresist with a new combination of focus and quantity of exposure.

5. A method of controlling a lithographic tool having a microscope and an exposure head for processing a wafer, the wafer having a coating of photoresist and comprising a plurality of fields each of which includes a product area, exposure of the photoresist via a reticle in said exposure head producing a latent image with verification marks in the photoresist, the method providing for an alignment of the wafer with the exposure head, the me&:hod comprising steps of:

exposing a number of said fields, one field at a time;

moving the wafer to said microscope, said microscope being operative to produce the detected image of the latent image by differential phase shift;

locating an overlay verification aid;

measuring average overlay values of offset in each of two dimensions for each of said number of fields;

correcting coordinates of said tool for a field position;

returning the wafer to said exposure head; and

exposing said photoresist with new overlay values.

6. A method of evaluating a bake cycle by use of a lithographic tool having a microscope and an exposure head for processing a wafer, the wafer having a coating of photoresist and being subjected to a bake cycle, exposure of the photoresist via a reticle in said exposure head producing a latent image with verification marks in the photoresist, said microscope being operative to produce a detected image of the latent image by differential phase shift, the method comprising:

prebaking the wafer;

exposing the entire wafer by said exposure head;

moving said wafer to a bake station;

placing said wafer on a heated vacuum chuck;

employing said microscope to measure the amplitude of points of said detected image;

evaluating dimensions of said verification marks in an overlay;

determining whether the amplitude of points of the detected image is sufficient to indicate adequate baking;

quenching the wafer by moving the wafer to a cooled platen; and

developing the photoresist.

7. A method of employing a lithographic tool to obtain latent image enhanced global alignment by use of verification marks and tool registration marks, the tool having a microscope and an exposure head for processing a wafer, the wafer having verification marks thereon and being coated with photoresist, exposure of the photoresist by a reticle in said exposure head producing a latent image with verification marks in the photoresist, said microscope being operative to produce a detected image of a latent image in the photoresist by differential phase shift, the method comprising steps of:

exposing registration and verification marks at a number of sites on the wafer;

employing the lithographic tool to locate the registration marks;

moving the wafer under said microscope;

locating and measuring overlay verification marks for each of said number of sites;

correcting locations of said registration marks by fitting a polynomial, the deriving translation, rotation, and magnification terms of the polynomial to determine corrective positioning of the entire wafer;

moving the wafer under said exposure tool;

using corrected fit to predict all site positions; and

exposing all sites of the wafer.

8. A method of controlling a lithographic tool having a microscope and an exposure head for processing a wafer, the wafer having a coating photoresist and comprising a plurality of dies, there being primary verification marks and tool registration marks located on the surface of said wafer, the method comprising steps of:

exposing said photoresist via a reticle in said exposure head to produce a latent image with secondary verification marks in the coating of photoresist;

observing a surface of said coating by use of said microscope, said microscope being operative to produce a detected image of the latent image by differential phase shift;

observing a surface of said coating by use of said microscope, said step of observing including a viewing of adjacent sites at a first location on said coating surface with separate beams of radiation to obtain data of said coating surface by differential phase shift induced on said beams by reflection from said coating surface, said step of observing also including a converting of said differential phase shift to amplitude data to produce an image point of said first location in said detected image;

repeating said observing step at additional locations on said coating surface spaced from said first location to obtain further image points in said detected image, all of said image points constituting said detected image;

wherein said observing step further comprises a step of illuminating said coating with radiation to which said coating is transparent to provide reflections from said coating surface and from an interface between said coating and said wafer, the reflections providing images of said primary and said secondary verification marks in said detected image; and

wherein said method further comprises:

correlating said detected image with reference images of verification marks to obtain a centroid of each of said verification marks; and

measuring the distance between the centroids to determine alignment of the wafer.
 Description Submit all comments and votes
 


BACKGROUND OF THE INVENTION

This invention relates to the construction of semiconductor devices and other layered devices by photolithography including steppers for displacing a semiconductor wafer relative to a mask or a reticle and, more particularly, to the use of latent images of alignment marks formed in a photoresist layer for increased precision in the locating of a wafer relative to a mask.

Numerous forms of semiconductor devices including integrated circuits, by way of example, are constructed by building up layers of material on a substrate, etching away portions of the material, followed by steps of deposition of other substances which may include dopants. The locations of the various materials are precisely controlled to insure an accurate formation of the various semiconductor structures. Typically, layers of photoresist are deposited and exposed by photolithographic apparatus including masks to delineate the forms, in two dimensions, of the desired structural elements. In the case of construction of numerous chips from a single wafer, a mask used in the construction of any one chip is also used for constructing the other chips. This is accomplished by stepping the wafer under an optical system including the mask for exposure of the individual wafer regions, or dies, of the respective chips. At each die, photoresist is exposed, typically with ultraviolet light by the optical system to form a latent image of the mask in a layer of photoresist. The wafer is then removed from the stepper, and developer is applied to the photoresist to develop the image. Etches selective to the development of exposed photoresist remove portions of the photoresist to prepare the wafer for the next stage of material deposition or other types of etching processes. At a later stage in the manufacture the wafer is returned to the stepper for exposure of the dies to another mask.

It is noted that the foregoing use of photolithographic apparatus in the printing of successive circuit patterns on the surface of a wafer can also be employed in the manufacture of reticles or masks is in the manufacture of semiconductor devices. Generally speaking, the use of the term mask is understood to include the term reticle or E-beam or maskless direct write control pattern for the purposes of the present invention.

To ensure accurate alignment of the wafer relative to the optical system, it is the practice in the initial stage of manufacture to produce tool registration aids on the wafer substrate in the marginal region surrounding each die, the registration aid being outside the product area of a die. A tool registration aid may be formed as a depression in the substrate surface, for example, wherein the aid is formed by an etch. A primary verification aid or mark may also be formed on the substrate. During subsequent steps in the manufacturing process, secondary verification marks located in the marginal region of a mask are projected onto a layer of photoresist and developed to allow alignment of the primary and the secondary verification marks.

The foregoing procedure presents a problem in that the verification marks imprinted in the photoresist must be observed in a manner which does not detract from the use of the photoresist in the process of imaging the details of an integrated circuit or other subject matter of the semiconductor device. Under present practice in which the verification marks imprinted on the photoresist are not usable until after the photoresist has been developed, the wafer is removed from the stepper, processed with a developing liquid, and then examined under a microscope to determine the degree of alignment between verification marks and registration marks. This wafer is known as a send ahead wafer, and must be reprocessed in the event that the alignment is poor. The stepper is then adjusted to correct the alignment, after which subsequent wafers can be processed by the stepper. The current practice is particularly inconvenient where relative few wafers are to be processed, and wherein frequent reticle changes may be required by a need to place several product patterns on a single wafer. The send-ahead wafer is a randomly selected product substrate from a batch. Alternatively, a monitor substrate which does not have a product being developed thereon may be employed to check alignment. In either case, the additional manufacturing steps represent a significant inconvenience.

SUMMARY OF THE INVENTION

The aforementioned problem is overcome and other advantages are provided by a manufacturing process employing a wafer stepper and photolithographic apparatus wherein, in accordance with the invention, a latent image of verification marks imprinted on a layer of photoresist is employed for alignment with registration marks previously produced on the substrate of a wafer. The invention is advantageous in that the latent image can be employed without the need for development of the exposed photoresist, thereby to preserve the latent image of subject matter for a product area on a die of the wafer. Therefore, alignment can be accomplished without removal of the wafer from the stepper. If inadequate alignment is found, the alignment can be corrected without removal of the wafer from the stepper with the result that only the first die, or a first plurality of dies, which dies have been exposed for the alignment process, have been lost while all the other dies on the wafer can now be exposed under conditions of correct alignment.

In accordance with a further embodiment of the invention, the latent image is viewed by an optical system employing illumination of the latent image with a photon energy lower than that required for exposure of the photoresist. Thereby, no alteration of the latent image occurs during the illumination. For example, where exposure of the photoresist to produce the latent image is accomplished by use of light in the deep ultraviolet region of the spectrum, the viewing of the latent image is accomplished with illumination with lower-frequency light in the near ultraviolet region of the spectrum.

In accordance with a further feature of the invention, examination of the latent image is accomplished with a microscope and further reticle elements operating in accordance with differential phase contrast, preferably Nomarski differential interference contrast. This produces a received beam of light in which changing depth and/or changing index of refraction of the photoresist layer produces an elliptically polarized wave which, upon being viewed through a polarization analyzer, produces variation in amplitude at the plane of a detector. The detector may be constructed as an array of charge-coupled devices (CCD) or a videcon which is scanned to extract data of a two-dimensional image at the plane of the detector. Variation in intensity across the detected image is stored as a set of pixels each represented as a multibit digital signal. The stored signal has at least several shades of gray to enable accurate observation of the blatant image.

An interesting feature of the optical processing by differential interference contrast (DIC) is the fact that the detected image shows a light region where the depth of the photoresist is decreasing and a dark region where the depth of the photoresist is increasing. Between these two regions, the image shows a medium value of gray. Exposure of the photoresist material to the ultraviolet radiation induces a slight decrease in thickness of the photoresist, and a change in the index of refraction. For example, a line having a width of two microns would appear in the detected image as a length of dark fringe spaced apart from a length of light fringe, the two fringes being spaced apart on centers by the foregoing width of two microns. The width of a fringe is a measure of the width of a transition region between the normal depth and refractive index, and the reduced thickness and altered refractive index.

In accordance with features of the invention, the foregoing characteristics of the DIC detected image permit convolution of the detected image and alignment with a reference image of verification marks to reduce the effect of noise on the determination of the precise location of the detected verification mark. Such noise results from, by way of example, deposits of aluminum and facets of polysilicon which may be present in the wafer. A comparison of the centroid of a detected secondary verification mark with the centroid of a primary verification mark produces a positional error signal which is used in connection with an error signal of a servomechanism of the stepper to refine the accuracy of the stepper. Similarly, the DIC detected image can be employed for enhanced global alignment in situations where verification marks for several dies are examined and averaged together to produce a position correction signal.

Also, in accordance with the invention, the strength of the detected image, specifically the intensity of a light or dark fringe, varies in accordance with the sharpness of focus of the exposing radiation. Therefore, examination of the detected image can be used to adjust the optical system for best focus. Furthermore, in view of the fact that the thickness and/or the refractive index of the exposed photoresist is dependent on the amount of exposure, namely the intensity and duration of the exposure, and is also dependent on the amount of heating in those photoresist materials which must be baked after exposure, examination of the detected image can also be used as a measure of exposure and a measure of baking.

It is to be noted that the theory of the invention for the measurement of parameters of the photoresist based on a viewing of a latent image in the photoresist is applicable to a variety of manufacturing situations in which a layer of photoresist is employed. The construction of multilayered semiconductor devices represents a common occurrence of a situation employing photoresist in the construction process. However, other important manufacturing situations, by way of example, relate to the configuration of ferroelectric materials in miniaturized recording heads, and the construction of masks and reticles used for constructing various devices. Accordingly, the methodology of the invention has applicability to diverse manufacturing processes, and is not limited to the construction of semiconductor devices. Nor is the invention limited to optical exposure tools but rather, encompasses E-beam, ion and X-ray exposure tools.

BRIEF DESCRIPTION OF THE DRAWING

The aforementioned aspects and other features of the invention are explained in the following description, taken in connection with the accompanying drawing wherein:

FIG. 1 shows a graphical representation of a typical patterned substrate with both plan and cross-sectional views of overlay patterns and latent image patterns, FIG. 1 being divided into four sections identified as FIGS. 1A-1D wherein FIG. 1A is a stylized view of a wafer, FIG. 1B is an enlarged view of one die of the wafer, FIG. 1C is an enlarged view of a square box-shaped primary verification mark surrounded by a similarly shaped secondary verification mark of a latent image, and FIG. 1D shows an L-shaped primary verification mark surrounded by an L-shaped secondary verification mark;

FIG. 2 is a diagrammatic view of optical equipment employed in the practice of the invention, the optical equipment including a modified Nomarski differential interference contrast (NDIC) microscope with autofocus and electro-optical phase modulator, the latter producing rotation of an optical connector;

FIG. 3 is a diagrammatic view of a measurement subsystem of the invention integrated with a standard step and repeat microlithographic exposure tool;

FIG. 4 shows an imaging detector output resulting from response of the NDIC latent image for the measurement of exposure dose, tool focus, and direct latent image line width measurement, FIG. 4 being presented in four sections as FIGS. 4A-4D, and wherein FIG. 4A shows variation in photoresist thickness with exposure, FIG. 4B shows a differential image for the geometry of FIG. 4A, FIG. 4C is a graph of image amplitude as a function of exposure dosage, and FIG. 4D is a graph of image amplitude as a function of focus;

FIG. 5 is a flow diagram for real-time in-situ exposure monitoring and control;

FIG. 6 is a flow diagram for real-time in-situ focus monitoring and control;

FIG. 6A is a flow diagram for direct measurement of latent image line-width;

FIG. 7 is a flow diagram for real-time in-situ overlay monitoring and control;

FIG. 8 is a diagrammatic view of a wire-frame, or reference pattern, used as a standard for convolution in an overlay position-determining algorithm, the view showing also representative results of a convolution calculation;

FIG. 9 is a stylized representation of successive steps employed in the formation of layers of material for the construction of a semiconductor device, such construction being advantageously implemented by the invention;

FIG. 10 is a diagrammatic view of a photoresist post-exposed bake thermal developer station;

FIG. 11 is a graphical representation of an NDIC image ratio as a function of bake time for a thermal developer station;

FIG. 12 is a graphical representation of tool grid and registration aid locations for blatant image enhanced global alignment; and

FIG. 13 is a flow diagram for latent image enhanced global alignment.

DETAILED DESCRIPTION

FIGS. 1A-1D describe alignment marks employed in the practice of the invention for aligning a wafer 20 with a reticle or mask in photolithographic apparatus to be described hereinafter. FIG. 1A discloses a set of six dies 22 by way of example, it being understood that, in practice, hundreds of dies may be present in a wafer. Global alignment marks 24 are provided for initial alignment of the wafer 20 upon placing the wafer within a stepper of the photolithographic apparatus.

In FIG. 1B, in stylized view, a portion of the wafer 20 of FIG. 1A has been enlarged to show a die 22 and a marginal region 26 surrounding the die 22. Two primary verification marks 28 and two tool registration marks 28B are arranged about the die 22, within the marginal region 26, and formed directly within a surface of the wafer 20. In the practice of the invention, during a manufacturing step wherein a photoresist layer is disposed upon the wafer 20, secondary verification marks provided by a reticle or mask are projected onto the layer of photoresist. Two such secondary verification marks 30 are shown in FIG. 1B. The verification marks 30 may have a desired configuration, such as a square-shaped picture frame as shown in FIG. 1B, or an L-shaped configuration as shown by an alternative primary verification mark 28A and an alternative secondary verification mark 30A in FIG. 1D. The verification mark 30 or 30A is substantially larger than and encloses the verification mark 28 or 28A so that, upon an initial alignment of the wafer 20 with the stepper, provided by the optical system of the stepper as will be described hereinafter, the primary verification mark 28 or 28A falls within the secondary verification mark 30 or 30A. While the secondary verification mark 30 or 30A is shown to be larger than the primary verification mark 28 or 28A, it is to be understood that the relative sizes may be reversed such that the secondary verification mark would be made smaller than the primary verification mark (not shown) with the latter enclosing the former.

FIG. 1C shows further details in the conduction of the registration and the verification marks 28 and 30. Therein, the corner portion of the picture frame in each of the marks has been deleted leaving four straight segments of marking arranged in the square configuration. The four mark segments in each of the verification marks 28 and 30 are sufficiently long so as to provide overlap between the corresponding mark segments of the verification marks 30 and 28 even upon displacement of the centroids of the marks relative to each other, as might occur upon initial alignment of the wafer with the stepper. An offset between the centroid positions, as measured in an X coordinate, of an X-Y coordinate system, is also shown in FIG. 1C.

As will be disclosed hereinafter, upon a viewing of the verification marks 28 and 30 by a scanning of a detected image along a coordinate axis, for example the X axis, edge lines of a mark segment are noted by a change of intensity in the detected image, this being a characteristic of the Nomarski differential interference contrast response of the microscope system employed in viewing the marks. Such an NDIC response is also indicated in FIG. 1C for the situation in which a scanning of the detected image is accomplished along a scan line parallel to the X axis and intersecting a portion of the verification mark 30 which is parallel to the Y axis.

FIG. 2 shows an optical system 32 employed by the invention for accomplishing a fine measurement of offset between primary and secondary verification marks, which fine measurement is to be employed by stepper positioning apparatus to accomplish a more accurate locating of the wafer within the stepper. The optical system 32 includes a source 34 of light, typically near ultraviolet, a condenser lens 36 for collimating rays of light from the source 34, and a rotator 38 of the electric vector of collimated light incident upon the rotator 38 from the lens 36. The rotator 38 comprises an electrooptic liquid crystal phase shifter which introduces phase shifts differentially to orthogonal components of the electric vector of the light incident upon the rotator 38 from the lens 36. The amount of differential phase shift is established in response to a voltage applied to the rotator 38 from a voltage controller 40. The output beam of light from the rotator 38 is indicated by line 42.

The optical system 32 further comprises a vidicon 44, a polarization analyzer 46, a half-silvered mirror 48 comprising a glass plate 50 with a layer 52 of silver disposed on a surface of the plate 50, a Nomarski modified Wollaston prism 54 comprising two prismatic elements 56 and 58 which meet along an interface 60, and a microscope objective 62. Also shown in FIG. 2 are components of a stepper 64, namely a stage 66 (shown in simplified form) for supporting the wafer 20 in front of the objective 62, and a servo unit 68 for positioning the stage 66 to align the wafer 20 in accordance with command signals developed by use of the optical system 32.

The vidicon 44 is provided by way of example as a detector of an image of subject matter of the wafer 20, it being understood that another form of area detector, such as a charge coupled device, may be employed instead of the vidicon 44. The vidicon 44 constitutes a part of an imager 70, the imager 70 further comprising scan control unit 72 and a digitizer 74 which are connected to the vidicon 44, and a memory 76 such as a random access memory connected to an output terminal of the digitizer 74. The scan control unit 72 directs the vidicon 44 to perform a raster scan of an image incident upon the vidicon 44 so as to enable the vidicon 44 to output data of the image as a sequence of scan frames each of which provides image data in the form of a sequence of scan lines. Data outputted by the vidicon 44 is sampled by the digitizer 74 and converted to a sequence of multibit digital words, for example, 8-bit words, which are applied to the memory 76 to be stored therein. An image/signal processor 78 which includes a computer 80 and timing circuitry 82 outputs timing signals for synchronizing operation of the scan control unit 72 and the digitizer 74. In addition, the processor 78 addresses the memory 76 for obtaining data from the memory 76. Furthermore, the processor 78 applies a signal to the voltage controller 40 for designating an amount of phase shift to provide a