Encapusalated electroluminescent phosphor particles and method for making same. The phosphor particles are encapsulated in a very thin oxide layer to protect them from aging due to moisture intrusion. The particles are encapsulated via a vapor phase hydrolysis reaction of oxide precursor materials at a temperature of between about 25.degree. C. and about 170.degree. C., preferably between about 100.degree. C. and about 150.degree. C. The resultant encapsulated particles exhibit a surprising combination of high initial luminescent brightness and high resistance to humidity-accelerated brightness decay.
CROSS-REFERENCE TO RELATED APPLICATIONS
This application is a continuation of application Ser. No. 07/912,786, filed Jul. 13, 1992, which is a division of application Ser. No. 07/514,440, filed Apr. 25, 1990, now U.S. Pat. No. 5,156,885.
Polymeric organic coating for electroluminescent lamp components, particularly for phosphor particles and electrodes and a method of making same, wherein the polymer is formed using an initiator, preferably by ring-opening metathesis polymerization. A dense hydrophobic organic coating is formed which is capable of protecting the electroluminescent device components from exogenous agents such as moisture and eventual degradation. The polymer layer may be attached to an outer surface of the component by one or more tethering layers.
Inorganic phosphor particles having a diamond-like carbon coating and the method of making these particles. Inorganic phosphor particles are coated with a diamond-like carbon coating, which can include additive components. The coating is applied in a plasma reactor process.
A method for making particles coated with a diamond-like network, which can include additive components. The method comprises subjecting a multiplicity of particles to a carbon-based plasma in an evacuated radio frequency powered capacitively coupled reactor system in which ion sheaths are formed around the electrodes and wherein the particles are agitated in such a manner as to expose their surfaces to the reactive species in the plasma while keeping the particles substantially within an ion sheath. The advantages of the present invention include (i) the efficient deposition of DLN onto particles at high deposition rates, (ii) the deposition of densely-packed DLN coatings, (iii) the ability to perform in situ surface cleaning of particles by ion bombardment with oxygen- and argon-containing plasmas prior to deposition of DLN, and (iv) the ability to tailor the bulk and surface properties of the coatings by manipulating the composition of the coating and the intensity of ion bombardment during the coating process.
Inorganic phosphor particles having a diamond-like carbon coating and the method of making these particles. Inorganic phosphor particles are coated with a diamond-like carbon coating, which can include additive components. The coating is applied in a plasma reactor process.
EL panels are made with PVDF/HFP copolymer resin binder, in substantially an un-crosslinked form, with DMAC solvent and/or other higher boiling point solvents/latent solvents/extenders. The resin binder is characterized by a melt viscosity of 1.0-8.5 kP using an industry standard test (ASTM D3835).
