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Process for making a granular detergent composition containing a selected crystalline calcium carbonate builder
   
Document Number
US Patent 6100232
Issued Date
August 8, 2000
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Abstract
A process for preparing a detergent composition is provided. The process involves: (a) continuously mixing a detergent surfactant paste and dry starting detergent material into a high speed mixer/densifier to obtain detergent agglomerates, wherein the ratio of the surfactant paste to the dry detergent material is from about 1:10 to about 10:1; and (b) mixing the detergent agglomerates in a moderate speed mixer/densifier to further densify and agglomerate the detergent agglomerates. The dry detergent material contains a builder which is a selected crystalline calcium carbonate material substantially having a rhombohedral crystalline structure with {1,0,-1,1} crystallographic indices.
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Number of Claims:
13
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Published
August 8, 2000
Application Number
09/033,210
Filed
March 2, 1998
US Classification
510/444   510/276 510/348 510/441
Int'l Classification
C11D   3/12   (20060101)   C11D   3/10   (20060101)   C11D   11/00   (20060101)  
Examiner
Parent Case
CROSS REFERENCE TO RELATED APPLICATIONS This application claims priority under Title 35, United States Code 119(e) from Provisional Application Ser. No. 60/040,165, filed Mar. 11, 1997.
USPTO Field of Search
510/444   510/441   510/276  
Related Patents
6576605 - Process for making a free flowing detergent composition - Owned by The Procter & Gamble Company (Cincinnati, OH)

A non-tower process for preparing a granular detergent composition, the process comprising the following steps: (i) fluidizing powder materials in a high-speed mixer/granulator having both a stirring action and a cutting action, the powder materials comprising: particulate solid water-soluble alkaline inorganic material in an amount in excess of that required for neutralization, optionally in admixture with one or more other particulate solids, and recycled fines, the powder materials having a total surface area; (ii) adding the liquid detersive materials to the high-speed mixer/granulator, the liquid detersive materials comprising: a liquid acid precursor, optionally in admixture with one or more other liquid materials, whereby neutralization of the acid precursor by the water-soluble alkaline inorganic material occurs; and (iii) granulating the mixture in the high-speed mixer/granulator to form detergent particles, wherein the ratio of the total surface area of the powder materials to the amount of liquid detersive materials in step (ii) is from about 0.02 to about 140.

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