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Method for trace water analysis in cyclic siloxanes useful as precursors for low dielectric constant thin films
   
Document Number
US Patent 7439318
Issued Date
October 21, 2008
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Inventors
Xu; Chongying (New Milford, CT)
Baum; Thomas H. (New Fairfield, CT)
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Abstract
An analytical technique for the accurate and precise measurement of trace water in chemical reagents, comprising the steps of combining a chemical reagent comprising .ltoreq.5 ppm water, with hexafluoroacetone (HFA), to form a sample mixture comprising at least the chemical reagent and a water derivative of hexafluoroacetone; and measuring the concentration of the water derivative of hexafluoroacetone by gas chromatography.
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Number of Claims:
20
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Published
October 21, 2008
Application Number
11/685,659
Filed
March 13, 2007
US Classification
528/483   436/39 436/72 528/491 528/493
Int'l Classification
G01N   25/56   (20060101)   C08F   6/06   (20060101)  
Examiner
Parent Case
CROSS-REFERENCE TO RELATED APPLICATION This is a continuation of U.S. patent application Ser. No. 10/107,885 filed Mar. 27, 2002, now U.S. Pat. No. 7,189,571 in the names of Alexander S. Borovik, Ziyun Wang, Chongying Xu and Thomas H. Baum for "METHOD FOR TRACE WATER ANALYSIS IN CYCLIC SILOXANES USEFUL AS PRECURSORS FOR LOW DIELECTRIC CONSTANT THIN FILMS," issued Mar. 13, 2007 as U.S. Pat. No. 7,189,571. The disclosure of said U.S. patent application Ser. No. 10/107,885 is hereby incorporated herein by reference, in its entirety. Priority is claimed under the provisions of 35 USC 120.
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