
A new form of .gamma.-- calcium pyrophosphate having a rhambohedral crystal shape and regular particle size, more especially in the range 8-81/2 microns, is prepared by controlled heating of anhydrous calcium hydrogen phosphate having a similar crystal form and particle size. The latter phosphate is prepared by precipitation of brushite and dehydration in an aqueous medium such as aqueous phosphoric acid at an elevated temperature. When the new pyrophosphate is employed as a source of calcium an...











